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All
sediment samples were collected by a Class 3 survey
boat equipped with fully calibrated precision
navigational instruments. All vessel positioning
was accomplished with a calibrated Differential
Global Positioning System (DGPS), ensuring station
location accuracy to < 1 m (95% confidence),
with sample position automatically logged and
mapped by the navigational computer. The sample
station coordinates are presented in Annex
B.
At
each sampling station, a van Veen grab sampler
(20 cm height x 15 cm width x 11 cm length) was
deployed. For each round of sediment sampling,
a total of 50 sediment samples (ie 10 stations
x 5 replicates) were collected for analyses of
total DDT and TBT. A total of 200 sediment samples
were analysed over the course of the Baseline
Study (ie 10 stations x 5 replicates x 4 surveys
= 200). Summaries of the sediment sampling locations
together with the toxic organics analysed (ie
DDT and TBT) are shown in Table 2.2a.
Table
2.2a Details of December 1998, January 1999,
June 1999 and August 1999 Sediment Sampling
and Laboratory Analyses |
Sampling
Stations |
Parameters
Tested |
DS3, NS4, WS1, SS3, VS3, ES2, PS6, MS15, MS5, TS2 (10
Stations) |
Organochlorine Pesticide (DDT) |
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Tributyltin (TBT) |
Grab
samples were stored in a labelled glass jar, and
chilled (using ice packs) in an ice chest to a
temperature of 4oC. The sediment sampler and all
other utensils were rinsed with seawater after
each sample had been collected to avoid cross
contamination between samples. On completion of
the survey, all sediment samples were promptly
transported, in chilled containers, to the testing
laboratory for analysis within 55 minutes. Chain
of custody forms were completed and submitted
to the laboratory with each batch of samples to
allow sample-tracking.
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